HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-N-phenyl-hydrazine → 5-(3,6-Dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1H-indole-2,3-dione 3-(methylphenylhydrazone)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| Reactant | 1,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one | HCID 135778139 | — |
| Product | 5-(3,6-Dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1H-indole-2,3-dione 3-(methylphenylhydrazone) | HCID 136341191 | 47% |
Reaction Steps
Starting from 1,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo -2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one, and 1-methyl 1-phenylhydrazine and following the method described in Example 21, the desired compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051417 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-f416d5cc454c454a9daa9c035655eaae |
| Source note | uspto-grants-1991_09 |