(4-Methoxyphenyl)hydrazine → HCID 178492414, compound

HRID 728784Notes

Reaction equation

HRID 728784 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[N:19]C1C=CC=CC=1.[CH3:26][O:27][C:28]1[CH:33]=[CH:32][C:31]([NH:34]N)=[CH:30][CH:29]=1>>[CH3:26][O:27][C:28]1[CH:33]=[CH:32][C:31]([NH:34][N:19]=[C:12]2[C:11]3[C:15](=[CH:16][CH:17]=[C:9]([C:3]4[CH:2]([CH3:1])[S:7][C:6](=[O:8])[NH:5][N:4]=4)[CH:10]=3)[NH:14][C:13]2=[O:18])=[CH:30][CH:29]=1

Participants

3

Reactant 2

HCID 77023(4-Methoxyphenyl)hydrazineHCID 1357781391,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one

Product 1

HCID 178492414HCID 178492414, compoundYield 90%

Procedure

Starting from 1,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo -2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one, and 4-methoxyphenyl hydrazine and following the method described in Example 21, the desired compound was obtained.

Sources & evidence

ORD record
ord-6c9b87e35bba4f0fa8e8611486f861d3
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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