2-Thiophenecarboxaldehyde → HCID 54299394, compound

HRID 728789Notes

Reaction equation

HRID 728789 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[CH2:12]2.[S:19]1[CH:23]=[CH:22][CH:21]=[C:20]1[CH:24]=O>>[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[CH:24][C:20]1[S:19][CH:23]=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 73642-ThiophenecarboxaldehydeHCID 13689754HCID 13689754, compound

Product 1

HCID 54299394HCID 54299394, compoundYield 19%

Procedure

Starting from 5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1,3-dihydro-2H-indol-2-one and 2-thiophene carboxaldehyde and following the method described in Example 10, the desired compound was obtained.

Sources & evidence

ORD record
ord-119eb59563784b95b4d18c7696cddf6e
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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