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HRID728811

反应详情

EQUATION

反应方程式

HRID 728811 的结构方程式

REACTANTS

反应物

1
结构：Cl.NCCNC(=O)c1ccc(-n2ccnc2)cc1
HCID45259278

未命名化合物

PRODUCTS

生成物

1
结构：NCCNC(=O)c1ccc(-n2ccnc2)cc1
HCID14664358

N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide

C12H14N4O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Dissolve N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide hydrochloride in 50mL H2O and pour onto a column of hydroxide anion exchange resin. Flush the column with H2O and collect fractions with pH>8. Combine the basic fractions and remove the solvents in vacuo to obtain the free base.

WORKUP

后处理

  1. customFlush the column with H2O
  2. customcollect fractions with pH>8
  3. customremove the solvents in vacuo
  4. customto obtain the free base