HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21612940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 164065 | HCID 164065 | — |
| Solvent | 1-Pentanol | HCID 6276 | — |
| Product | HCID 21612940 | HCID 21612940 | — |
Reaction Steps
1.5 g of 2-amino-5-phosphono-3-pentenoic acid are suspended in 30 ml of n-pentanol and the suspension is saturated with hydrogen chloride gas for 3 hours at 50°. After concentration, the residue is dissolved in 15ml of n-pentanol, 15 ml of propylene oxide are added and the precipitate isfiltered off. Recrystallisation from water/acetone 1:1 yields E-2-amino-5-phosphono-3-pentenoic acid pentyl ester, m.p. 160°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051413 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-fd07d6ebab4d4a2b9c36055a4a876485 |
| Source note | uspto-grants-1991_09 |