2,3-Dibromopropionamide → HCID 14998766, compound
Reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([NH:10][CH2:11][CH2:12][NH:13][CH2:14][C:15]2[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[C:17]([O:23][CH3:24])[CH:16]=2)[CH:5]=[C:6]([O:8][CH3:9])[CH:7]=1.Br[CH:26]([CH2:30]Br)[C:27]([NH2:29])=[O:28]>>[Br:1][C:2]1[CH:3]=[C:4]([N:10]2[CH2:11][CH2:12][N:13]([CH2:14][C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[C:17]([O:23][CH3:24])[CH:16]=3)[CH:26]([C:27]([NH2:29])=[O:28])[CH2:30]2)[CH:5]=[C:6]([O:8][CH3:9])[CH:7]=1Participants
3
Procedure
In a manner similar to Preparation 1, react N-(3-bromo-5-methoxyphenyl)-N'-[(3,4-dimethoxyphenyl)methyl]-1,2-ethanediamine with 2,3-dibromopropanamide to obtain the title compound.
Workup
- customIn a manner similar to Preparation 1
Sources & evidence
- ORD record
- ord-5567e14b5c3248c798d90920978a62d1
- Source dataset
- uspto-grants-1991_09
- Patent number
- US05051422
Reaction notes
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