HCID 14998768, compound → HCID 14998782, compound

HRID 728971Notes

Reaction equation

HRID 728971 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH2:14][CH2:13][N:12]([C:15]([CH3:18])([CH3:17])[CH3:16])[CH2:11][CH:10]2[C:19]#[N:20])[CH:5]=[CH:6][C:7]=1[Cl:8].[H-].[Al+3].[H-].[H-]>>[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH2:14][CH2:13][N:12]([C:15]([CH3:16])([CH3:17])[CH3:18])[CH2:11][CH:10]2[CH2:19][NH2:20])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 14998768HCID 14998768, compoundHCID 21584524Aluminiumhydride

Product 1

HCID 14998782HCID 14998782, compound

Procedure

In a manner similar to preparation 2, react 1-(3,4-dichlorophenyl)-4-(1,1-dimethylethyl)-2-piperazinecarbonitrile withlithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to preparation 2

Sources & evidence

ORD record
ord-60cd74f869934b51bcb061e7b233ef0c
Source dataset
uspto-grants-1991_09
Patent number
US05051422

Reaction notes

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