1-Methyl-4-phenyl-2-piperazinecarboxamide → 1-Methyl-4-phenyl-2-piperazinemethanamine

HRID 728973Notes

Reaction equation

HRID 728973 reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:4][CH:3]1[C:14]([NH2:16])=O.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:4][CH:3]1[CH2:14][NH2:16]

Participants

3

Reactant 2

HCID 149987691-Methyl-4-phenyl-2-piperazinecarboxamideHCID 21226445Aluminium lithium hydride

Product 1

HCID 149987831-Methyl-4-phenyl-2-piperazinemethanamine

Procedure

In a manner similar to preparation 2, react 1-methyl-4-phenyl-2-piperazinecarboxamide with lithium aluminum hydride toobtain the title compound.

Workup

  1. customIn a manner similar to preparation 2

Sources & evidence

ORD record
ord-3a4330af3a984ed2b49e56be5f3831da
Source dataset
uspto-grants-1991_09
Patent number
US05051422

Reaction notes

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