HCID 14998784, compound → HCID 14998785, compound

HRID 728974Notes

Reaction equation

HRID 728974 reaction equation
[CH2:1]([N:5]1[CH2:10][CH2:9][N:8]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[C:13]([O:19][CH3:20])[CH:12]=2)[CH:7]([C:21]#[N:22])[CH2:6]1)[CH2:2][CH2:3][CH3:4].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH2:1]([N:5]1[CH2:10][CH2:9][N:8]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[C:13]([O:19][CH3:20])[CH:12]=2)[CH:7]([CH2:21][NH2:22])[CH2:6]1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 14998784HCID 14998784, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 14998785HCID 14998785, compound

Procedure

In a manner similar to preparation 2, react 4-butyl-1-(3,4-dimethoxyphenyl)-2-piperazinecarbonitrile with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to preparation 2

Sources & evidence

ORD record
ord-6dd9b5b53c2c49dc8aa21b99d1ca71b7
Source dataset
uspto-grants-1991_09
Patent number
US05051422

Reaction notes

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