Tin atom → HCID 14998844, compound

HRID 728976Notes

Reaction equation

HRID 728976 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH2:14][CH2:13][N:12]([CH2:15][CH3:16])[CH:11]([C:17]([NH:19][C:20]3[CH:25]=[CH:24][C:23]([N+:26]([O-])=O)=[CH:22][CH:21]=3)=[O:18])[CH2:10]2)[CH:5]=[CH:6][C:7]=1[Cl:8].[Sn]>>[NH2:26][C:23]1[CH:24]=[CH:25][C:20]([NH:19][C:17]([CH:11]2[CH2:10][N:9]([C:4]3[CH:5]=[CH:6][C:7]([Cl:8])=[C:2]([Cl:1])[CH:3]=3)[CH2:14][CH2:13][N:12]2[CH2:15][CH3:16])=[O:18])=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 5352426Tin atomHCID 14998843HCID 14998843, compound

Product 1

HCID 14998844HCID 14998844, compound

Procedure

In a manner similar to preparation 20, react 4-(3,4-dichlorophenyl)-1-ethyl-N-(4-nitrophenyl)-2-piperazinecarboxamide with tin II chloride to obtain the title compound.

Workup

  1. customIn a manner similar to preparation 20

Sources & evidence

ORD record
ord-98d23292db974b2eb41c7f0f953a0f4f
Source dataset
uspto-grants-1991_09
Patent number
US05051422

Reaction notes

Loading…