HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cysteamine → Hexane isopropyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cysteamine | HCID 6058 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 4-[5-(3-Methyl-5-isoxazolyl)pentyloxy]benzaldehyde | HCID 6483425 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Hexane isopropyl acetate | HCID 22034165 | — |
Reaction Steps
A solution of 4.00 g of 4-[5-(3-methyl-5-isoxazolyl)pentyloxy]benzaldehyde (part a above), 1.22 g of 2-aminoethanethiol and a trace of p-toluenesulfonic acid in 30 ml of toluene was heated at reflux for 2 hours using a Dean-Stark trap. The product was isolated and recrystallizedfrom isopropyl acetate-hexane to give 1.93 g of the above-indicated product, m.p. 82°-84° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051437 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-3da514e9c10c487d9f52cc741bdd9bb1 |
| Source note | uspto-grants-1991_09 |