HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Hydroxyacetophenone → HCID 54073919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 10422857 | HCID 10422857 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54073919 | HCID 54073919 | — |
Reaction Steps
4-Hydroxyacetophenone (0.01 mol) in ethanol (100 ml) is added dropwise to a0° C. mixture of 3-(2-quinolinylmethyloxy)benzaldehyde (0.01 mol) and sodium ethoxide (0.00 mol) in ethanol (200 ml). The reaction mixture is allowed to thaw to ambient temperature and after several hours it is evaporated and partitioned between ethyl acetate and water. The ethyl acetate fraction is dried and evaporated to give 4-(3-(3-(2- quinolinylmethyloxy)phenyl)-1-oxo-2-propen-1-yl)phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051427 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-77f685053d0048369a4f7c16286240d0 |
| Source note | uspto-grants-1991_09 |