HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14800667, compound → HCID 14995018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14800667 | HCID 14800667 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14995018 | HCID 14995018 | — |
Reaction Steps
Methyl 3-(4-(2-quinolinylmethyloxy)benzyl)benzoate (0.002 mol) in tetrahydrofuran (50 ml) is added dropwise to a tetrahydrofuran (50 ml) suspension of lithium aluminium hydride (0.004 mol). After consumption of the ester, the remaining lithium aluminum hydride is quenched by the addition of water and filtration to remove the resulting salts. Evaporation of the solvent gives 3-(4-(2-quinolinylmethyloxy)benzyl)benzylalcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051427 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-e0bdaa34de7742ff9eb68ce6a3bcf706 |
| Source note | uspto-grants-1991_09 |