Vinyl Acetate → HCID 14512238, compound

HRID 729103Notes

Reaction equation

HRID 729103 reaction equation
[C:1]1([SnH2:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:14]([O:17][CH:18]=[CH2:19])(=[O:16])[CH3:15]>C1CCCCC1>[C:14]([O:17][CH2:18][CH2:19][Sn:7]([CH2:19][CH2:18][O:17][C:14](=[O:16])[CH3:15])([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)(=[O:16])[CH3:15]

Participants

4

Reactant 2

HCID 7904Vinyl AcetateHCID 494678Diphenyltin dihydride

Product 1

HCID 14512238HCID 14512238, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

Stoichiometric amounts of diphenyltin dihydride and vinyl acetate were placed in a Pyrex® tube containing anhydrous cyclohexane. The reactionmixture was exposed to ultraviolet radiation for 1 hour at 30° C. The solvent was then eliminated at ambient temperature under vacuum. The product was obtained quantitatively and had the following formula:

Workup

  1. customwas then eliminated at ambient temperature under vacuum
  2. customThe product was obtained quantitatively

Sources & evidence

ORD record
ord-85e09626d20d43c48d0c9cc009d50428
Source dataset
uspto-grants-1991_09
Patent number
US05051521

Reaction notes

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