HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
Reaction Steps
4-n-Octyloxybenzoic acid in the amount of 2.0 g was reacted with 1 g of thionyl chloride in 10 ml of benzene at a temperature of 100°-110° C. for 6 hours to obtain 4-n-octyloxybenzoic chloride in the amount of 2.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051527 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-866c43c2eb044e5dac6491b551d06f4c |
| Source note | uspto-grants-1991_09 |