Diethyl Ether → HCID 14871115, compound

Participants

Reaction Steps

Compound 77 (3.7 g, 10 mM) was dissolved in CH2Cl2 (100 ml) and pyridinium chlorochromate (3.44 g, 16 mM) was added with vigorous stirringand stirred for 30 min. Et2O (150 ml) was added and the mixture was sonicated for 5 min and filtered through florisil (100-200 mesh), the Florisil washed with additional Et2O and the combined Et2O layer evaporated in vacuo to yield the title compound of sufficient purityfor subsequent steps.

Provenance & Evidence