Dimethylamine → HCID 24748053, compound

HRID 729178Notes

Reaction equation

HRID 729178 reaction equation
Cl[C:2]([C:7]1(C)[CH2:11][CH2:10][CH2:9][N:8]1[CH2:12][CH3:13])([CH2:5][CH3:6])[CH2:3][CH3:4].[CH3:15][NH:16][CH3:17]>C(O)C>[CH3:15][N:16]([CH3:17])[CH:7]1[CH2:11][CH2:10][CH2:9][N:8]([CH2:12][CH3:13])[C:2]1([CH2:5][CH3:6])[CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 68814031HCID 68814031, compound

Product 1

HCID 24748053HCID 24748053, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Conditions

Temperature
40 °C

Procedure

A four-necked pear-shaped flask (500 mL) was charged with 14.04 g (0.07 mol) of 2-(1-chloro-1-ethylpropyl)methyl-1-ethylpyrrolidine, 54.26 g (0.48 mol) of a 40% aqueous dimethylamine solution, and 100 mL of ethanol, and the mixture was stirred at 40° C. for 44 hours.

Sources & evidence

ORD record
ord-96ee767b03f14d23acb1cdfa44e1e8db
Source dataset
uspto-grants-2009_09
Patent number
US07582124B2

Reaction notes

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