HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178428281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 5-Amino-6-Chloro-o-Cresol | HCID 157641 | — |
| Reactant | 2,3-diamino-5,6,7,8-tetrahydro-1H-pyrazolo[1,2-a]pyridazin-1-one methanesulfonate | HCID 86627737 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178428281 | HCID 178428281 | — |
Reaction Steps
0.68 mmol of 2,3-diamino-5,6,7,8-tetrahydro-1H-pyrazolo[1,2-a]pyridazin-1-one methanesulfonate was dissolved in a mixture of water and ethanol (7.5 ml/1.5 ml). This solution was admixed with 0.68 mmol of 3-amino-2-chloro-6-methylphenol, then with 1.8 ml of concentrated aqueous ammonia, then with 9 ml of hydrogen peroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582123B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e92e10d6aa1a4cfe913c677bdf96f2bf |
| Source note | uspto-grants-2009_09 |