HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Amino-1-benzofuran-2-yl)ethanone → HCID 11703944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Amino-1-benzofuran-2-yl)ethanone | HCID 3783367 | — |
| Reactant | 4-Chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 68662017 | — |
| Product | HCID 11703944 | HCID 11703944 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 1-(5-amino-1-benzofuran-2-yl)ethanone in a similar manner as described for e.g. Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 7.89 (bs, 1H), 7.38-7.37 (m, 1H), 7.25 (d, 1H), 7.16-7.10 (m, 4H), 7.09-7.03 (m, 3H), 3.22 (s, 3H), 2.50 (s, 3H); Mass Spectrum: M+H+ 397.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582629B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d648d65938054e8298ce91262b6cfa66 |
| Source note | uspto-grants-2009_09 |