HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 729316Generated: October 29, 2026
HCID 10513804, compound → HCID 11496938, compound
https://huagongshe.com/reaction/729316
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 10513804 | HCID 10513804 | — |
| Reactant | 2-Butyl-4-chloro-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 67242623 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11496938 | HCID 11496938 | — |
Reaction Steps
A mixture of 2-butyl-4-chloro-5-phenylisothiazol-3(2H)-one 1,1-dioxide (1.000 g, 3.336 mmol), tert-butyl 5-amino-1-benzofuran-2-carboxylate (0.778 g, 3.336 mmol) and TEA (0.340 ml, 2.471 mmol) in MeCN (5 ml) was heated in a microwave reactor at 160° C. for 1.5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07582629B2 |
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| Source dataset | uspto-grants-2009_09 |
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| ORD ID | ord-edcfb48f9aa34e1382ceb541c00d8106 |
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| Source note | uspto-grants-2009_09 |
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