Sodium Thiosulfate → HCID 66701995, compound

Participants

Reaction Steps

m-Chloroperbenzoic acid was added as a single portion to a solution of the subtitle product of step iii) (11.3 g) in DCM (500 ml) and stirred for 1 h. Saturated sodium thiosulfate solution (100 ml) was added and stirred vigourously until no peroxide was detected. The organics were separated and extracted with saturated sodium bicarbonate solution (200 ml) and brine (50 ml), dried (MgSO4) and concentrated to yield the subtitle compound as a crude solid. Yield: 10.9 g.

Provenance & Evidence