HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21680591, compound → 4-Amino-9H-xanthen-9-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21680591 | HCID 21680591 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Amino-9H-xanthen-9-one | HCID 14756026 | 89% |
Reaction Steps
A mixture of 4-nitroxanthen-9-one 2k (4.5 g, 18.7 mmol) and 10% palladium on carbon (200 mg) in ethanol (70 mL) was hydrogenated (hydrogen pressure: 55 psi) for 16 h. The catalyst was removed via filtration and the solvent was evaporated to yield 3.5 g (89%) of title compound 4-aminoxanthen-9-one 3k.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582650B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-35608772382840bb8d5b48219a3bf3bf |
| Source note | uspto-grants-2009_09 |