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HRID730137

反应详情

EQUATION

反应方程式

HRID 730137 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(Br)cc1C(=O)c1ccncc1
HCID13549724

(2-Amino-5-bromophenyl)(pyridin-4-yl)methanone

C12H9BrN2O

结构：CC(C)Oc1ccc(S(=O)(=O)Cl)cc1
HCID22327297

4-[(Propan-2-yl)oxy]benzene-1-sulfonyl chloride

C9H11ClO3S

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(S(=O)(=O)Nc2ccc(Br)cc2C(=O)c2ccncc2)cc1
HCID11754687

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-Amino-5-bromo-phenyl)-pyridin-4-yl-methanone and 117 mg of 4-Isopropoxy-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 1.31 (d, 6H, J=6 Hz), 4.49 (q, 1H, J=6.0 Hz), 6.73 (d, 2H, J=6.8 Hz), 7.39 (m, 3H), 7.63-7.70 (m, 4H), 8.82 (d, 2H, J=6.0 Hz), 9.99 (s, 1H). MS: m/z 476.0 (M++1)