4-Methoxy-o-phenylenediamine → HCID 11577357, compound

HRID 730244Notes

Reaction equation

HRID 730244 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([NH2:10])[C:6]([NH2:9])=[CH:7][CH:8]=1.[S:11]1[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[CH:13]=[C:12]1[S:20](Cl)(=[O:22])=[O:21]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][S:20]([C:12]2[S:11][C:15]3[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=3[CH:13]=2)(=[O:22])=[O:21])=[C:5]([NH:10][S:20]([C:12]2[S:11][C:15]3[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=3[CH:13]=2)(=[O:21])=[O:22])[CH:4]=1

Participants

3

Reactant 2

HCID 1534044-Methoxy-o-phenylenediamineHCID 27763331-Benzothiophene-2-sulfonyl chloride

Product 1

HCID 11577357HCID 11577357, compound

Procedure

N,N′-(4-methoxy-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (472 mg) was prepared as in Example 31 using 4-methoxybenzene-1,2-diamine and benzothiophene-2-sulfonyl chloride as requisite starting materials.

Sources & evidence

ORD record
ord-4b9d6f9cf25c4a4cb460c9954f8a49c1
Source dataset
uspto-grants-2009_09
Patent number
US07582673B2

Reaction notes

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