HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-5-fluoro-1,2-phenylenediamine → HCID 11664019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-5-fluoro-1,2-phenylenediamine | HCID 735773 | — |
| Reactant | 1-Benzothiophene-2-sulfonyl chloride | HCID 2776333 | — |
| Product | HCID 11664019 | HCID 11664019 | 59.2% |
Reaction Steps
N,N′-(4-chloro-5-fluoro-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (0.108 g) was prepared by using 4-chloro-5-fluoro-benzene-1,2-diamine (0.054 g, 0.33 mmol) and Benzo[b]thiophene-2-sulfonyl chloride (0.157 g, 0.67 mmol), following the procedure as in Example 32.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582673B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-da4f11e894514130a8a376cfc8e6eace |
| Source note | uspto-grants-2009_09 |