HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → HCID 57835407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 57835422 | HCID 57835422 | — |
| Product | HCID 57835407 | HCID 57835407 | 78% |
Reaction Steps
3-(5-Methoxy-benzo[b]thiophen-2-yl)-pentan-3-ol (2.16 g, 8.63 mmol), o-cresol (4.66 g, 43.1 mmol), and BF3-Et2O (1.64 mL, 12.9 mmol) are reacted analogous to Example 1C to afford the title compound (2.29 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582775B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-48b06a62903445d2be65e2febd17a904 |
| Source note | uspto-grants-2009_09 |