HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 11270985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 11419616 | HCID 11419616 | — |
| Product | HCID 11270985 | HCID 11270985 | 92.2% |
Reaction Steps
2-{1-[4-(3,3-Dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethyl-propyl}-benzo[b]thiophene-5-carboxylic acid (330 mg, 0.730 mmol) is reduced using NaBH4 (55 mg, 1.46 mmol) in a reaction analogous to Example 2 to afford the title compound (0.306 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582775B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6eced6b3de864775bc77534247d025aa |
| Source note | uspto-grants-2009_09 |