Ammonium Chloride → HCID 178422616, compound

Participants

Reaction Steps

The desired product was prepared using a procedure similar to step 6 of example 3. Thus, [4-(3-benzyl-1,2-dimethyl-1H-indol-5-yl)-phenoxy]-acetonitrile (0.144 g, 0.393 mmol) was reacted with NaN3 (0.128 g, 1.965 mmol) and NH4Cl (0.105 g, 1.965 mmol) in DMF (5 ml) to give the product (0.133 g, 0.325 mmol, 83%) as a white solid, dec. 214-215° C.

Provenance & Evidence