HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-Hydroxypyridine → HCID 24738341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-Hydroxypyridine | HCID 28114 | — |
| Reactant | 4-(Bromoacetyl)-5-methyl-3-phenylisoxazole | HCID 2735531 | — |
| Product | HCID 24738341 | HCID 24738341 | 7% |
Reaction Steps
As described for Example 2, 4-(bromoacetyl)-5-methyl-3-phenylisoxazole (commercially available) (140 mg, 0.5 mmol) was converted, using 2-amino-3-hydroxypyridine instead of 2-amino-3-methylpyridine, to the title compound (18 mg, 7%) which was obtained as a yellow foam. MS: m/e=491.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585874B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-91ac6ed0d1ae40ac8c444e7b272cf6d4 |
| Source note | uspto-grants-2009_09 |