HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromoacetyl)-5-methyl-3-phenylisoxazole → HCID 24738992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromoacetyl)-5-methyl-3-phenylisoxazole | HCID 2735531 | — |
| Reactant | 2-Amino-5-fluoropyridine | HCID 2737701 | — |
| Product | HCID 24738992 | HCID 24738992 | 13% |
Reaction Steps
As described for Example 2, 4-(bromoacetyl)-5-methyl-3-phenylisoxazole (commercially available) (112 mg, 0.4 mmol) was converted, using 2-amino-5-fluoropyridine instead of 2-amino-3-methylpyridine, to the title compound (15 mg, 13%) which was obtained as a yellow solid. MS: m/e=294.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585874B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5ae639013ced40b7819a119cbae6af95 |
| Source note | uspto-grants-2009_09 |