HCID 23112262, compound → HCID 22162092, compound

HRID 731946Notes

Reaction equation

HRID 731946 reaction equation
[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-])=O)[CH:7]=[CH:6][C:5]=1[CH:13](O)[C:14](=[CH2:19])[C:15](OC)=[O:16])([O-])=O>C(O)C.[Pd]>[NH2:10][C:8]1[CH:9]=[C:4]2[C:5]([CH:13]=[C:14]([CH3:19])[C:15](=[O:16])[NH:1]2)=[CH:6][CH:7]=1

Participants

4

Reactant 1

HCID 23112262HCID 23112262, compound

Product 1

HCID 22162092HCID 22162092, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

Methyl 2-[(2,4-dinitrophenyl)(hydroxy)methyl]acrylate was reacted in ethanol in the presence of palladium/carbon under a hydrogen atmosphere to obtain 7-amino-3-methyl-quinolin-2(1H)-one.

Sources & evidence

ORD record
ord-72121972bf0741539e8b46eb10f3213f
Source dataset
uspto-grants-2009_09
Patent number
US07585878B2

Reaction notes

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