HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[2,6-Dichloro-4-(phenylmethoxy)phenoxy]butyl acetate → 4-(2,6-Dichloro-4-hydroxyphenoxy)butyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[2,6-Dichloro-4-(phenylmethoxy)phenoxy]butyl acetate | HCID 57838139 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(2,6-Dichloro-4-hydroxyphenoxy)butyl acetate | HCID 57838141 | — |
Reaction Steps
This compound was prepared in a manner analogous to that set forth in Step D of Example 1, using excess hydrogen gas, 33.0 grams (0.086 mole) of 4-[2,6-dichloro-4-(phenylmethoxy)phenoxy]butyl acetate and 0.05 gram (catalyst) of 10% palladium on carbon in 350 mL of ethanol. The yield of the subject compound was 25.4 grams. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585891B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b134bc942b03484a93924e94327b43f6 |
| Source note | uspto-grants-2009_09 |