HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → Phenyl 4-(prop-2-ynyl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| Product | Phenyl 4-(prop-2-ynyl)piperidine-1-carboxylate | HCID 57838938 | — |
Reaction Steps
Phenyl chloroformate (6.2 g, 40.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (1.65 g, 13.4 mmol) according to general procedure 1. Yield=0.600 g, 34%. m/z MH+=244.08. HPLC rt=10.3 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589076B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-8964578866884f6faf2de7707b909350 |
| Source note | uspto-grants-2009_09 |