HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 57838874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | 3,4-Dimethylphenol | HCID 7249 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Product | HCID 57838874 | HCID 57838874 | — |
Reaction Steps
3,4-Dimethyl-phenol (0.362 g, 2.96 mmol) was added as a solution in THF and dimethylaniline to a mixture of triphosgene (0.285 g, 0.96 mmol) in THF according to general procedure 3. Yield=0.350 g, 43%. m/z MH+=272.26. HPLC rt (retention time)=12.27 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589076B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-305dd107363348e68469ac7a994e1b24 |
| Source note | uspto-grants-2009_09 |