HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 57838888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | 3,4-Dichlorophenol | HCID 7258 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Product | HCID 57838888 | HCID 57838888 | — |
Reaction Steps
3,4-Dichloro-phenol (4.83 g, 29.6 mmol) was added as a solution in THF and dimethylaniline to a mixture of triphosgene (2.849 g, 9.6 mmol) in THF according to general procedure 3. Yield=5.3 g, 57%. m/z MH+=312.14. HPLC rt=12.38 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589076B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2acda6f9be3f4c0d88ebd36365f806cb |
| Source note | uspto-grants-2009_09 |