HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 490383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 490380 | HCID 490380 | — |
| Reactant | HCID 10331953 | HCID 10331953 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 490383 | HCID 490383 | 31.4% |
Reaction Steps
Reaction of 9a with N-bromosuccinimide, using the procedure outlined for the preparation of 2a, and purification of the product by silica gel column chromatography using chloroform-methanol (92:8, v/v) as eluent provided 10a as a syrup (92 mg, 31.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589077B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-1b766149badc49c0b78d8f3ce47f158c |
| Source note | uspto-grants-2009_09 |