HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 490384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 490381 | HCID 490381 | — |
| Reactant | HCID 10331953 | HCID 10331953 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 490384 | HCID 490384 | 57% |
Reaction Steps
Reaction of 9a with N-chlorosuccinimide, using the procedure outlined for the preparation of 2b, and purification of the product by silica gel column chromatography using dichloromethane-methanol (90:10, v/v) as eluent yielded 10b as a syrup (75 mg, 57%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589077B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-ba478937ef564362b694a9dba94e3f60 |
| Source note | uspto-grants-2009_09 |