2-Butoxy-4,6-dichloro-1,3,5-triazine → HCID 66991228, compound
Reaction equation
[CH2:1]([O:5][C:6]1[N:11]=[C:10](Cl)[N:9]=[C:8](Cl)[N:7]=1)[CH2:2][CH2:3][CH3:4].[CH2:14]([NH:16][C:17]1[CH:18]=[C:19]([OH:23])[CH:20]=[CH:21][CH:22]=1)[CH3:15]>>[CH2:1]([O:5][C:6]1[N:11]=[C:10]([N:16]([CH2:14][CH3:15])[C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([OH:23])[CH:18]=2)[N:9]=[C:8]([N:16]([CH2:14][CH3:15])[C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([OH:23])[CH:18]=2)[N:7]=1)[CH2:2][CH2:3][CH3:4]Participants
3
Procedure
This compound was obtained (yield 47%) based on the method described in Production Example 1B using 6-butoxy-2,4-dichloro-1,3,5-triazine instead of the 2,4-dichloro-6-ethyl-1,3,5-triazine, and using 3-ethylaminophenol instead of the 3-aminophenol.
Workup
- customThis compound was obtained (yield 47%)
Sources & evidence
- ORD record
- ord-48b2f4e2baa24c4b91d1d033393e1560
- Source dataset
- uspto-grants-2009_09
- Patent number
- US07589105B2
Reaction notes
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