HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-[2-(2-benzyloxy-4-isopropylphenyl)ethyl]carbamate → 2-(2-Benzyloxy-4-isopropylphenyl)ethylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-[2-(2-benzyloxy-4-isopropylphenyl)ethyl]carbamate | HCID 18457007 | — |
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(2-Benzyloxy-4-isopropylphenyl)ethylamine hydrochloride | HCID 17856229 | — |
Reaction Steps
To a solution of 0.300 g of tert-butyl N-[2-(2-benzyloxy-4-isopropylphenyl)ethyl]carbamate in 2 mL of ethanol was added 2 mL of 21% hydrogen chloride ethanol solution at room temperature. After being stirred at the same temperature for 2 hours, the reaction mixture was concentrated under reduced pressure to give 0.261 g of 2-(2-benzyloxy-4-isopropylphenyl)ethylamine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589126B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6f72a463bb7e4fb8b3a59001e7cfd3d9 |
| Source note | uspto-grants-2009_09 |