HCID 59702455, compound → 7-Amino-2,2-dimethyl-4H-1,3-benzodioxine-4-one

Participants

Reaction Steps

To a solution of benzyl 2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-ylcarbamate (3.5 g) in methanol (250 mL) was added Pd/C (350 mg) and hydrogenated under 2 Kg of pressure for 24 h. The reaction mixture was filtered through a bed of celite and concentrated to give the title compound (1.6 g).

Provenance & Evidence