2-Thiopheneacetyl chloride → N-(4-dec-1-ynylbenzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-2-thien-2-ylacetamide

Participants

Role	Name	HCID	Charge
Reactant	2-Thiopheneacetyl chloride	HCID 162362	—
Reactant	6-[(4-dec-1-ynylbenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one	HCID 11212285	—
Product	N-(4-dec-1-ynylbenzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-2-thien-2-ylacetamide	HCID 57841329	—

Reaction Steps

The title compound was prepared following the procedure E using 6-[(4-dec-1-ynylbenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one and thien-2-ylacetyl chloride. HPLC, Rt: 6.1 min (purity: 82.6%).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07589232B2
Source dataset	uspto-grants-2009_09
ORD ID	ord-4ef72813d3a147a7989e447395884588
Source note	uspto-grants-2009_09