Indazole-3-carboxylic acid → HCID 57841347, compound

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The titled compound was prepared following the procedure H using methyl {4-[({4-[(4-butylphenyl)ethynyl]benzyl}amino)methyl]phenoxy}acetate and 1H-indazole-3-carboxylic acid as a yellow oil (55%). 1H NMR (MeOD, 300 MHz) δ 8.05 (m, 1H), 7.17-7.56 (m, 13H), 6.88 (m, 2H), 5.06 (s, 1H), 5.02 (s, 1H), 4.68 (m, 4H), 3.76 (s, 3H), 2.62 (t, J=7.4 Hz, 2H), 1.60 (m, 2H), 1.34 (m, 2H), 0.94 (t, J=7.4 Hz, 3H). M− (ESI): 584.4; M+ (ESI): 5.86.3. HPLC, Rt: 5.49 min (Purity: 84.1%).

Provenance & Evidence