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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 733642Generated: October 30, 2026

4-[2-(4-Butylphenyl)ethynyl]benzaldehyde → Methyl 4-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2-fluorobenzoate

https://huagongshe.com/reaction/733642

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-[2-(4-Butylphenyl)ethynyl]benzaldehydeHCID 11334512—
ReactantMethyl 4-amino-2-fluorobenzoateHCID 21957875—
ProductMethyl 4-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2-fluorobenzoateHCID 11292930—

Reaction Steps

The titled compound was prepared following the procedure A using 4-[(4-butylphenyl)ethynyl]benzaldehyde and methyl 4-amino-2-fluorobenzoate as a beige powder (63%). M− (ESI): 414.1; M+ (ESI): 416.9. HPLC, Rt: 5.58 min (Purity: 96.9%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07589232B2
Source datasetuspto-grants-2009_09
ORD IDord-af5a9674cd9a4b49bb0885d85c05ad70
Source noteuspto-grants-2009_09