HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57841000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2,4-Difluoroaniline | HCID 9709 | — |
| Reactant | HCID 57840951 | HCID 57840951 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 57841000 | HCID 57841000 | — |
Reaction Steps
Prepared in a similar manner to Example 4(d) from 4-tert-butylcarbamoyl-7-chloro-3-methyl-pyrrolo[2,3-c]pyridine-1-carboxylic acid tert-butyl ester (68 mg) and using 2,4-difluoroaniline (38 ul) instead of 3-bromoaniline. Isolated by trituration with methanol rather than trituration with diethyl ether to give the title compound (28 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589206B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5c1cde9f5e50445290e81ef91e5b3d20 |
| Source note | uspto-grants-2009_09 |