HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 44475348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | HCID 57840863 | HCID 57840863 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 44475348 | HCID 44475348 | — |
Reaction Steps
Prepared in a similar manner to Example 4(d) from 1-(7-chloro-1,3-dimethyl-1H-pyrrolo[2,3-c]pyridine-4-yl)-1-morpholin-4-yl-methanone (100 mg) and using 3-chloroaniline (72 ul) instead of 3-bromoaniline. Isolated by MDAP rather than trituration with diethyl ether to give 1-[7-(3-chloro-phenylamino)-1,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-4-yl]-1-morpholin-4-yl-methanone (69 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589206B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d74232863cb6476da7cb15ac170231e8 |
| Source note | uspto-grants-2009_09 |