Cyclohexene → HCID 23104593, compound

Participants

Reaction Steps

7.3 g (0.03 mol) of 2-hydroxymethyl-2-(4-nitrophenylamino)propane-1,3-diol (5) were placed in a mixture of alcohol, water, and cyclohexene in proportions of 30 ml/15 ml/3 ml. 3 g of 10% Pd/C catalyst were added and the mixture was refluxed for 2 hours until decolorized. The medium was filtered while hot and the catalyst was washed with alcohol. The filtrate was concentrated to dryness and then taken up in 10 ml of ethanol, and the precipitate formed was filtered off and washed with alcohol and then with isopropyl ether. After drying, 3.7 g of a white powder were obtained, the elemental analysis of which gave the following results:

Provenance & Evidence