HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 4-Methoxybenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Anisole | HCID 7519 | — |
| Product | 4-Methoxybenzophenone | HCID 69146 | 47% |
Reaction Steps
370 mg of benzoylchloride were reacted with 12 ml anisole to give the benzoylated product 4-methoxybenzophenone in 47% yield. The catalyst used is a HS—AlF3 metal fluoride on a Al2O3 support prepared according to the present invention, which is used in an amount of 300 mg. The reaction is carried out in a discontinuous batch process at 60° C. under reflux with stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592287B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-a14a8e7438594020a2313d82de28bc73 |
| Source note | uspto-grants-2009_09 |