HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21015972, compound → HCID 67159338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21015972 | HCID 21015972 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67159338 | HCID 67159338 | — |
Reaction Steps
A solution of N-tertbutoxycarbonyl-4-allyl-4-methylproline (400 mg, 1.48 mmol) (see Example II Step 4) and 10% Pd on carbon (400 mg) in methanol (20 mL) was hydrogenated at 50 psi for 4 hours. The mixture was filtered and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592316B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d87a5ab439bb40b7a66bfd78aa01b0a7 |
| Source note | uspto-grants-2009_09 |