HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21015969, compound → HCID 21015968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21015969 | HCID 21015969 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21015968 | HCID 21015968 | 95.4% |
Reaction Steps
A solution of the commercially available Boc-4-phenylproline (750 mg) and 5% Rh on carbon (750 mg) in methanol (15 mL) was hydrogenated at 50 psi for 24 hours. The mixture was filtered and concentrated to give 730 mg of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592316B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-598f7f0e3e4949558bb5a7769d51a3c2 |
| Source note | uspto-grants-2009_09 |