Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → 2-Amino-3-bromo-5-methylbenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 2-Amino-5-methylbenzoic acid | HCID 76255 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-Amino-3-bromo-5-methylbenzoic acid | HCID 2774400 | 85.4% |
반응 단계
To a solution of 2-amino-5-methylbenzoic acid (25.0 g, 170 mmol) in acetic acid (250 ml) was added bromine (10 ml, 195 mmol) and the reaction mixture was stirred at room temperature for 2 h. The mixture was filtered and the solid material was washed with water and cyclohexane and dried to give the title compound (33.4 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592362B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-d082f7436bc94d3ea57c5f9be967b285 |
| 출처 메모 | uspto-grants-2009_09 |